化学合成。
医药
合成路线 1（1. 合成：170911-92-9）
产率：100%
合成条件：With hydrogen In methanol; ethyl acetate for 2 h;
实验步骤：将Pd / C 10％（0.3％p / p）加入到4-（4-硝基苯基）哌嗪-1-羧酸叔丁酯（1当量）的混合物（1：1比例）MeOH：EtOAc（0.03）中的溶液中。M）。 向反应容器中的气氛中加入H 2（1臂），剧烈搅拌反应2小时。 此时，将反应混合物通过硅藻土垫过滤并真空浓缩，得到标题化合物（定量）; MS（ES +）m / z 278（M + H）+
参考文献：
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