化学合成,用于制造染料及颜料。
化学合成; 染料及颜料制造
合成路线 1(1. 合成:4857-04-9)
产率:93%
合成条件:With hydrogenchloride In waterReflux
实验步骤:通用方法:将适当的1,2-二氨基苯衍生物(0.1mol)和适当的羧酸衍生物(0.15mol)在100ml 5N HCl中的混合物加热至回流并搅拌3-5小时。 将反应混合物冷却至室温后,用碳酸氢钠中和。 通过抽滤过滤形成的沉淀,用水洗涤并干燥。
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