157327-41-8 1-Boc-3-[(二甲氨基)亚甲基]-4-氧代哌啶

WGK Germany:WGK 3 海关编码:2933399990 存储类别:11 - 可燃固体

作为医药中间体，用于相关药物合成。

医药

合成路线 1（1. 合成：157327-41-8）

产率：100% 合成条件：at 80℃; for 24 h; 实验步骤：将N，N-二甲基甲酰胺二甲基缩醛（18g，20mL，151mmol）和1-（叔丁氧基羰基）哌啶-4-酮（30g，151mmol）在DMF（240mL）中的混合物在80℃下搅拌。 °C，持续24小时。 将混合物真空浓缩，得到标题化合物，为黄色固体（38.4g，100％）。 MS（ESI，阳离子）m / z：255 [M + H] +。 参考文献：

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