化学合成。
化学合成
合成路线 1（1. 合成：808-57-1）
产率：90.1%
合成条件：at 25℃; for 24 h;
实验步骤：根据Synthesis，477,1994和JP-A-8-119894中描述的方法合成2,3,6,7,10,11-六羟基三亚苯基一水合物的B型晶体。 即，将1,2-二甲氧基苯（31.78g，0.23摩尔）和无水氯化铁（120g，0.74摩尔）溶解在70％硫酸中，并在搅拌下使溶液在25℃反应24小时。 反应完成后，将溶液倒入冰水（500g）中，过滤收集沉淀的晶体。 将所得晶体用水（1L）洗涤后，干燥，得到浅紫色2,3,6,7,10,11-六甲氧基三亚苯（28.2g，理论收率1,2-二甲氧基苯：90.1％） （Synthesis，477,1994的方法）。
参考文献：
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