53087-13-1 3-苄氧基溴苯

合成路线 2（2. 合成：53087-13-1）

产率：100% 合成条件：With potassium carbonate In acetone for 15 h; Reflux 实验步骤：向3-溴苯酚（3g，17.34mmol）的丙酮（100mL）溶液中加入苄基溴（2.2mL，19.07mmol）和K 2 CO 3（7.0g，52.02mmol），并将所得混合物回流15小时。。 将反应混合物冷却至室温，过滤，并用丙酮洗涤。 浓缩滤液，通过硅胶色谱法纯化，得到标题化合物（白色固体，5.1g，100％收率）。 1 H NMR（300MHz，CDCl 3）δ7.50-7.30（m，5H），7.20-7.01（m，3H），6.98-6.80（m，1H），5.05（s，2H）。 参考文献：

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