化学合成。
化学合成
合成路线 1（1. 合成：18733-91-0）
产率：96%
合成条件：Stage #1: With n-butyllithium In tetrahydrofuran at -78℃; for 2 h; Inert atmosphere Stage #2: at -78 - 20℃; for 14 h; Inert atmosphere
实验步骤：将1,4-二溴苯（10g，42.4mmol）加入到氮气流-78℃的THF（100ml）中，从2.5M n-BuLi（16.9ml，42.4mmol）缓慢搅拌2小时，然后， 在搅拌12小时后，在-78℃下将二氯二苯基硅烷（4.9g，19.3mmol）在室温下缓慢搅拌2小时。 EA用水提取反应，然后用MgSO 4干燥，浓缩，得到有机硅胶柱，重结晶，得到9.2g所需化合物（96％）。
参考文献：
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