概述
4-溴-2-甲氧基苯酚 是一种生化试剂，可作为生物材料或有机化合物，用于生命科学相关研究。
生化试剂; 生物材料; 有机化合物; 生命科学研究
合成路线 1（1. 合成：7368-78-7）
产率：95%
合成条件：With tetra-N-butylammonium tribromide In dichloromethane at 23℃; for 2 h;
实验步骤：一般步骤：将NBu4Br3（1.0当量）在CH 2 Cl 2（~5mL / mmol NBu 4 Br 3）中的溶液立即加入到苯酚1（1.0当量）的CH 2 Cl 2溶液（~5mL / mmol 1）中。 将反应混合物在23℃下搅拌2小时。 减压（12毫巴，40℃）除去溶剂。 将水（5.0mL）加入到残余物中，水层用Et 2 O（3×10mL）萃取。 分离有机层并干燥（MgSO 4）。 在减压下（14毫巴，40℃）除去有机溶剂，得到油状残余物，将其通过吸附色谱法（SiO 2，CH 2 Cl 2）纯化。
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