化学合成。
化学合成
合成路线 1（1. 合成：2444-90-8）
产率：95%
合成条件：With sodium hydroxide; potassium carbonate In water at 100℃; for 1 h;
实验步骤：将0.01摩尔双酚A，0.02摩尔NaOH和150毫升10％K 2 CO 3水溶液加入250毫升三颈烧瓶中，鼓入氮气以除去烧瓶中的氧气。使混合物在100℃下反应1小时，得到沉淀物。在氮气氛下滤出沉淀物，用30mL热异丙醇洗涤两次，然后在200℃下减压干燥3小时，得到25.8g双酚A双钠盐。产率为95percent;实施例27;将0.01摩尔双酚A，0.02摩尔NaOH和150毫升35％K 2 CO 3水溶液加入250毫升三颈烧瓶中，鼓入氮气以除去烧瓶中的氧气。使混合物在100℃下反应1小时，得到沉淀物。在氮气氛下滤出沉淀物，用30mL热异丙醇洗涤两次，然后在200℃下减压干燥3小时，得到25.8g双酚A双钠盐。产率为95percent。
参考文献：
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