化学合成。
化学合成
合成路线 1（1. 合成：74733-30-5）
产率：92%
合成条件：With tert.-butylhydroperoxide; cetyltrimethylammonim bromide; potassium bromide In water at 120℃; Microwave irradiation
实验步骤：一般步骤：将反应混合物在受控微波合成仪（Biotage Initiator + SP Wave型，0-200W，2.45GHz，稳定状态下加热至60W）下处理数分钟（反应在1巴压力下达到120℃））。 使用EtOAc-己烷梯度通过柱色谱分离最终产物
参考文献：
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