79670-17-0 5-溴-2-溴甲基苯甲酸甲酯

危险性质：非危险化学品

化学合成。

医药中间体

合成路线 1（1. 合成：79670-17-0）

产率：97% 合成条件：With N-Bromosuccinimide; dibenzoyl peroxide In tetrachloromethane at 85℃; for 2 h; 实验步骤：将5-溴-2-甲基苯甲酸甲酯（1g，4.4mmol），N-溴代琥珀酰亚胺（0.80g，4.4mmol），过氧化苯甲酰（56mg，0.23mmol）的四氯化碳（20mL）混合物在85℃下搅拌。 °C 2小时。 将混合物通过硅胶垫过滤并真空浓缩，得到所需产物（1.3g，97％收率）。 ESI-MS m / z：306.0 [M + H] +。 参考文献：

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