化学合成。
化学合成
合成路线 1（1. 合成：75581-11-2）
产率：97%
合成条件：With N-iodo-succinimide; bis(trifluoromethanesulfonyl)imidategold(I) In dichloromethane; toluene at 20℃; for 14 h;
实验步骤：一般步骤：向搅拌的底物（1mmol）的CH 2 Cl 2或（CH 2 Cl）2（0.1M）溶液中加入Ph3PAuNTf2（0.025mmol，19mg;络合物Ph3PAuNTf2甲苯，2：1），然后加入N-碘代琥珀酰亚胺（1.1）。 mmol，248mg）。 将所得溶液在室温下搅拌。 或在回流下直至原料完全转化。 在减压下除去溶剂后，通过快速柱色谱法使用不同梯度的己烷和EtOAc纯化粗物质，得到纯的所需产物。
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