化学合成。
化学合成
合成路线 1（1. 合成：1207-72-3）
产率：97%
合成条件：With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 2 h; Cooling with ice
实验步骤：称取NaH（60％纯度，1.0g，25.1mmol）在冰水浴中缓慢加入50ml圆底瓶的DMF（10ml）中，随后加入碘甲烷（1.3g，11.04mmol）和化合物吩噻嗪。 （2g，10.0mmol），转移至室温搅拌2h，TLC监测反应后，加水，用DCM（50ml×3）萃取，硫酸镁干燥，然后浓缩干燥，用硅胶柱1a分离产物（2.1 g），白色固体，熔点：96℃，产率97％。
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