化学合成；分析试剂，HPLC衍生化试剂。
医药中间体；化学合成；分析试剂（HPLC衍生化试剂）
合成路线 1（1. 合成：5000-65-7）
产率：100%
合成条件：With phenyltrimethylammonium tribromide In tetrahydrofuran at 20℃; for 1 h;
实验步骤：在室温下向搅拌的澄清的1-（3-甲氧基苯基）乙酮（20nL，139mmol）的四氢呋喃（250mL）黄色溶液中分批加入三溴化苯基三甲基铵（54.7g，145mmol）并搅拌1小时。 然后，滤出铵盐，滤饼用乙醚洗涤。 减压浓缩滤液，得到的油状产物无需进一步纯化，得到2-溴-1-（3-甲氧基苯基）乙酮（32.6g，142mmol，定量收率）。
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