化学合成。
化学合成
合成路线 1（1. 合成：5460-29-7）
产率：88.3%
合成条件：With tetrabutylammomium bromide In N,N-dimethyl-formamide at 70℃; for 2 h;
实验步骤：50mLDMF，0.025mol邻苯二甲酰亚胺钾盐，0.10mol 1,3-二溴丙烷和0.5g TBAB，70反应2.0h;冷却至室温，倒入冰水乙酸乙酯萃取，洗涤，干燥，溶解，静置过夜，5.91g 将N-（3-溴丙基）邻苯二甲酰亚胺沉淀，为白色固体，mp 70-73°C，收率88.3％。
参考文献：
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