3163-27-7 1-溴甲基萘

合成路线 2（3. 合成：3163-27-7）

产率：80% 合成条件：With tribromo-isocyanuric acid In ethyl acetate for 6 h; Reflux; Green chemistry 实验步骤：通用程序：将芳烃（2.0mmol）和TBCA（0.25g，0.68mmol）的EtOAc（20mL）溶液在搅拌下回流6小时。 在反应结束时，然后通过过滤分离沉淀的氰尿酸，并将滤液在减压下蒸发至干。 将残余物通过短色谱柱（SiO 2，用15：1己烷 - 乙酸乙酯洗脱），得到纯化的产物。 参考文献：

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