化学合成。
化学合成; 有机合成
合成路线 1（1. 合成：583-70-0）
产率：97%
合成条件：With N-Bromosuccinimide In 1,2-dichloro-ethane at 60℃; for 10 h; Sealed tube
实验步骤：通用程序：将NBS（1.0mmol）和催化剂1（基于底物的0.1或1mol％Au）称入10mL密封容器中，然后加入DCE（2mL）和底物（1.0mmol）。 将反应在所需温度下搅拌指定的时间。 反应后，用磁铁除去催化剂，减压浓缩溶液，用柱色谱法纯化。
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