化学合成。
化学合成
合成路线 1(1. 合成:6223-78-5)
产率:100%
合成条件:With hydrogenchloride In water
实验步骤:使用Bruson H等人,J Am Chem Soc,62:36(1940)中所述的已知方法合成2,5-二氯-2,5-二甲基己烷(化合物2),其中50g 2,5- 使用二甲基己烷-2,5-二醇(化合物1)和1L浓盐酸。 定量测量产率。 化合物2的性质与Bruson等人报道的相匹配。
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