化学合成。
化学合成
合成路线 1（1. 合成：626-01-7）
产率：93%
合成条件：With sodium tetrahydroborate In ethanol; water at 20℃; for 1.50 h;
实验步骤：通用方法：将TAPEHA-Pd（0.015g）加入到硝基芳烃（1.0mmol）的EtOH /水（1/1）（20mL）溶液中。 将NaBH 4（4.0mmol）缓慢加入混合物后，反应混合物的颜色在几分钟内逐渐变黑，导致形成钯纳米颗粒（TAPEHA-PdNPs）。 在室温和大气压下搅拌1.5小时后，通过过滤除去催化剂，用3×30mL EtOAc萃取适体。 将合并的有机层用MgSO 4干燥并真空浓缩。
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