化学合成。
化学合成
合成路线 1（1. 合成：454-81-9）
产率：100%
合成条件：With hydrogen In ethanol at 40℃;
实验步骤：描述7. 2-氨基-4-（三氟甲基）苯酚。（D7）; 将2-硝基-4-（三氟甲基）苯酚（100mg，0.483mmol）的乙醇（10mL）溶液泵送通过H-立方体（TM）。 氢化器CatCart（Pd / C，30×4mm），流速为1mL / min，温度为40℃，压力为40psi，在低压下用甲醇（10×1mL）补充溶液。 将收集的溶液蒸发至干，得到灰白色固体（88mg，假定定量收率）。 该物质无需进一步纯化即可继续使用。（M + H）+ = 178.1HNMRδ（CDCl 3）：6.76（1H，d，J = 8.4Hz），6.94（1H，d，J = 8.4Hz）， 6.98（1 H，s）。
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