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C9H8N2257.2 °C (760 mmHg)溶解度0.786 mg/ml ; 0.00545 mol/l 酸度系数pKa1.40±0.30 (Predicted) 条件: 100℃反应0.05小时,无溶剂( neat),使用10 wt%硫酸化多硼酸盐催化剂。收率: 98%参考文献: [1] Journal of Chemical Sciences, 2017, vol. 129, #2, p. 141-148 [2] Heteroatom Chemistry, 2012, vol. 23, #5, p. 472-477 [3] Tetrahedron Letters, 2011, vol. 52, #49, p. 6597-6602 [4] Chinese Chemical Letters, 2011, vol. 22, #6, p. 753-756 [5] Patent: US2007/179144, 2007, A1. Location in patent: Page/Page column 4 [6] Synthesis (Germany), 2013, vol. 45, #11, p. 1546-1552 [7] Patent: WO2006/127458, 2006, A2. Location in patent: Page/Page column 112 [8] Patent: WO2006/133381, 2006, A2. Location in patent: Page/Page column 7 [9] Patent: US2006/264631, 2006, A1. Location in patent: Page/Page column 37 [10] Patent: US2006/270848, 2006, A1. Location in patent: Page/Page column 39 [11] Chemische Berichte, 1884, vol. 17, p. 320 [12] Justus Liebigs Annalen der Chemie, 1887, vol. 237, p. 334 [13] Chemische Berichte, 1884, vol. 4, p. 220,221 [14] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982, p. 357-364 [15] Russian Journal of General Chemistry, 1997, vol. 67, #2, p. 285-294 [16] Justus Liebigs Annalen der Chemie, 1887, vol. 237, p. 339 [17] Justus Liebigs Annalen der Chemie, 1896, vol. 292, p. 246