713-52-0 3-羟基-4-硝基苯甲酸甲酯

运输信息：常温运输。危险描述：非危险化学品，具有刺激性（Irritant），海关编码2918290090。

作为有机合成中间体和医药中间体，主要用于实验室研发过程和化工生产过程中。

有机合成中间体; 医药中间体

路线1：

• 步骤：将3-羟基-4-硝基苯甲酸（10）（5.10g，27.85mmol）溶解在MeOH（43mL）中并冷却至0℃，缓慢加入SOCl₂（3.20mL，43.69mmol），将反应混合物在回流条件下搅拌17小时，将残留的油状物再溶解在MeOH中并浓缩（4x以除去过量的SOCl₂），得到标题化合物（5.49g，27.85mmol，定量），为黄色固体。
• 条件：0℃；17小时；回流；惰性气氛
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